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Molybdenum Vacuum Heat Treat Furnace

Vacuum Furnace

Molybdenum Vacuum Heat Treat Furnace

Item Number : KT-VM

Price varies based on specs and customizations


Max. temperature
1400 ℃
Heating rate
0-10℃/min
Temperature control accuracy
±1℃
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Molybdenum Vacuum Furnace: Precision High-Temperature Processing

A molybdenum vacuum furnace is a specialized high-temperature heat treatment system engineered for demanding industrial and laboratory applications. It employs robust molybdenum foil as its heating element and operates within a controlled vacuum environment to safeguard materials from contamination. This design ensures exceptional high-temperature stability, superior vacuum performance, efficient thermal transfer, and long-term durability, making it ideal for processes where material purity and precise atmospheric control are paramount.

Key Features & Benefits

  • Superior High-Temperature Stability: Guarantees consistent heating temperatures (up to 1400 °C) for reliable and repeatable heat treatment processes, even under the most demanding operational conditions.
  • Exceptional Vacuum Integrity: Maintains a high, clean vacuum level, effectively preventing contamination and ensuring the purity and integrity of the materials being processed.
  • Optimized Thermal Efficiency: The molybdenum heating elements facilitate rapid heating rates and excellent thermal uniformity throughout the chamber, enhancing overall process efficiency and throughput.
  • Robust and Durable Construction: Engineered with high-quality molybdenum components that exhibit excellent resistance to extreme temperatures and oxidation, ensuring prolonged furnace life and minimizing maintenance.

Detail & Parts

Molybdenum plate of heat insulation material in vacuum furnace

Molybdenum plate of heat insulation material in vacuum furnace
Molybdenum plate of heat insulation material in vacuum furnace
Molybdenum plate of heat insulation material in vacuum furnace

Small thermal expansion; High melting point; High thermal conductivity.

Technical Specifications

Furnace model KT-VM
Max. temperature 1400 ℃
Constant work temperature 1300 ℃
Chamber insulation material molybdenum heat shield
Heating element Molybdenum Strip
Heating rate 0-10℃/min
Temperature sensor Build in S type thermal couple
Temperature controller Touch screen PID controller with PLC
Temperature control accuracy ±1℃
Temperature uniformity ±5℃
Electric power supply AC110-440V,50/60HZ
Standard Chamber Sizes Stocks
Chamber size (mm) Effective volume (L) Chamber size (mm) Effective volume (L)
150x150x200 4.5 400x400x500 80
200x200x300 12 500x500x600 125
300x300x400 36 600x600x700 253
Custom design sizes and volume are accepted. Inquire about your custom requirements.

Versatile Applications

The molybdenum vacuum furnace is extensively used across various high-tech fields, including but not limited to:

  • Vacuum sintering of metals and ceramics
  • Vacuum brazing of complex assemblies
  • Sapphire crystal growth and annealing
  • Specialized brazing operations
  • Advanced heat treatment processes
  • Casting of precision aircraft components
  • Refining of high-purity metals and alloys
  • Production of electrodes for remelting
  • Powder roasting and calcination
  • Ceramic sintering and densification
  • High-temperature material experiments
  • Critical material treatment under vacuum
  • High-temperature atmosphere sintering (with appropriate modifications)
  • Ceramic glue discharge and debinding
  • Flue gas treatment research
  • Annealing and sintering processes requiring stringent atmospheric control

Operating Principle

The molybdenum vacuum furnace leverages the exceptional high-temperature resistance and vacuum compatibility of molybdenum foil. This foil serves as both the heating element and furnace liner. The system operates by creating a high-temperature vacuum environment through resistive heating of the molybdenum foil. This design effectively isolates the processed materials from external contaminants and allows for precise temperature control, crucial for high-temperature heat treatment processes in a clean, controlled atmosphere.

Advanced Safety Systems

  • Kindle Tech vacuum furnaces are equipped with over-current protection and over-temperature alarm functions; the furnace will automatically shut off power if limits are exceeded.
  • An integrated thermocouple detection function monitors sensor integrity; the furnace will stop heating and trigger an alarm if a thermocouple break or failure is detected.
  • Features a power failure restarting function, allowing the furnace to resume the heating program automatically once power is restored after an outage.

Optional Configurations

Enhance your furnace to meet specific experimental needs with options such as:

  • Independent furnace temperature monitoring and recording systems
  • RS 485 communication port for PC remote control and data exporting
  • Pneumatic vacuum valve linkage with the temperature controller for automated operation
  • Advanced touch screen temperature controller with versatile, operator-friendly functions
  • Cold water circulation cooling machine for efficient furnace shell jacket cooling

Partner with KINTEK for Your High-Temperature Furnace Needs

Leveraging exceptional R&D and in-house manufacturing, KINTEK provides diverse laboratories with advanced high-temperature furnace solutions. Our product line, including Muffle, Tube, Rotary Furnaces, Vacuum & Atmosphere Furnaces (like this Molybdenum Vacuum Furnace), and CVD/PECVD/MPCVD Systems, is complemented by our strong deep customization capability to precisely meet unique experimental requirements.

Ready to find the perfect furnace solution or need a custom design? Our team of experts is here to assist you. Contact KINTEK today to discuss your project or request a quote!

Precautions and Maintenance

The molybdenum foil vacuum furnace consists of key components such as the furnace chamber, molybdenum strips, vacuum gauge, vacuum system, and water cooler. The following precautions and maintenance guidelines should be observed to ensure optimal performance and longevity:

Furnace Chamber
  • Regularly inspect the chamber’s interior surface for brightness.
  • Ensure dryness and cleanliness inside the chamber to prevent oxidation and product contamination.
  • Avoid rapid heating rates that may cause thermal expansion deformation of the insulation screen.
  • Verify the leak rate and ultimate vacuum before initiating heating.
  • Maintain a vacuum in the chamber when not in use, and perform chamber baking if volatiles are present.
  • Implement a slower heating rate during high-temperature stages.
Molybdenum Strips Heater
  • Handle with care; do not drop objects onto the molybdenum strips when removing products, as it may cause breakage.
  • Prevent low-melting point iron-containing products from volatilizing onto the molybdenum strips, as it can lead to strip melting and breakage over time.
  • Securely hold the product with both hands or appropriate tools when taking it out.
  • Strictly control the impurity content in the product.
Pirani Gauge and Ionisation Gauge
  • Adhere to safety regulations for electrical equipment when operating and maintaining pirani gauges.
  • Avoid forcibly disassembling the gauge tubes while the furnace is under vacuum.
  • Do not pressurize the gauge (above 0.05Pa); if necessary, turn off the gauge power.
  • Refrain from introducing corrosive gas atmospheres.
  • Calibrate the vacuum gauge with dry air or nitrogen, as other atmospheres may cause measurement deviations.
  • Avoid turning on the ionization gauge under atmospheric pressure, as it may result in damage.
  • Clean the seals and contact surfaces with acetone or alcohol when disassembling, and apply vacuum grease before reassembling.
  • Perform zero point and full-scale calibration for the first use or after a period of use to match the vacuum and pirani gauges.
Mechanical Pump
  • Ensure the pump temperature does not exceed 45 degrees to prevent non-wear of the pump cavity and detrimental effects on the vacuum.
  • Monitor the oil color in the oil window regularly.
  • Check for oil splashing from the exhaust when starting the vacuum pump, and inspect the oil level.
  • Measure the pump temperature before and during operation, and monitor the cooling water temperature.
  • Change the oil every three months (model: HFV-100).
  • If the oil level is high, open the drain valve to lower it to the standard level.
Roots Pump
  • Maintain cleanliness inside the pump cavity.
  • Monitor the quality of pump oil.
  • Ensure proper pump rotation.
  • Avoid placing products with high moisture or large particles in the furnace chamber.
  • Promptly replace the diffusion pump oil if it becomes discolored or emulsified.
  • Immediately contact the manufacturer if any abnormal conditions occur with the pump.
Diffusion Pump
  • Check if the diffuser oil in the oil window requires replacement.
  • Monitor the pumping speed after starting.
  • Ensure adequate cooling water supply to the pump.
  • Replace the diffusion pump oil with the appropriate model (HFV-3).
  • Verify that the heater temperature, oil level, and pump core installation are normal.
  • Maintain the pump surface temperature between 10-35 degrees Celsius and humidity below 65%.
Water Cooler
  • Thoroughly read the manual before operating the water cooler.
  • Pay attention to the rotation directions of the inlet and outlet water pumps.
  • Confirm that the furnace water inlet pressure is displayed correctly after starting.
  • Establish an effective heat dissipation system.
  • Regularly check the water quality inside the water tank.
  • Clean the heat dissipation system every 3-5 months.
  • Avoid overloading the set temperature; for example, if the set temperature is 20 degrees, it should not go below 21 degrees. Adjust the set point above 21 degrees.
  • Ensure proper ventilation for the cooler’s placement.
  • Occasionally open the side cover and clean the inside water tank with diluted hydrochloric acid.

In summary, the molybdenum foil vacuum furnace is an efficient, stable, durable, and safe device. Diligent adherence to regular vacuum maintenance, safe operation protocols, and preventative maintenance practices are essential for ensuring its long-term stable operation and maximizing your return on investment.

FAQ

What Are The Main Applications Of A Vacuum Furnace?

Vacuum furnaces are primarily used for vacuum quenching (tempering, annealing) to achieve desired material properties, vacuum brazing for welding below the base metal's melting point, vacuum sintering to bond metal powder grains into parts, and vacuum plus magnetism for metal and magnetic material treatment. They are also widely used in semiconductor devices, optical thin films, functional coatings, nanomaterials, and other fields, providing important technical support for material preparation and functional improvement.

What Is An Atmosphere Furnace Used For?

Atmosphere furnaces are widely used in material processing, metal processing, semiconductor manufacturing, solar cell production, optical materials, ceramics and glass industry, electronic material manufacturing, and research and development of new energy materials.

What Are The Main Applications Of A Horizontal Vacuum Furnace?

Horizontal vacuum furnaces are primarily used for: 1. Annealing: Softening materials to improve ductility. 2. Sintering: Bonding particles to form solid structures. 3. Brazing: Joining materials using a filler metal. 4. Heat Treatment: Altering material properties through controlled heating and cooling. They are also used for heat treatment of metals and alloys, manufacturing electronic components, processing composite materials and ceramics, and sintering metals and ceramics.

What Is A Vacuum Induction Furnace?

A vacuum induction furnace is a specialized heating device that melts metals in a vacuum environment using induction heating technology. It is designed to remove impurities and improve the quality of the melted metals by preventing oxidation and contamination.

What Are The Key Features Of A Vacuum Furnace?

A vacuum furnace heats materials, mostly metals, at extremely high temperatures with low pollution and high consistency. Materials can be loaded vertically or horizontally. Vacuum furnaces can have batch or continuous designs, depending on cooling medium, load size, temperature, and pressure. They come in hot wall and cold wall designs, with cold wall furnaces offering higher operating temperature ranges, faster heating and cooling, and greater temperature uniformity.

What Are The Key Features Of An Atmosphere Furnace?

The key features of an atmosphere box furnace include its ability to maintain a specific gas environment, such as inert gases (e.g., nitrogen, argon), reducing gases (e.g., hydrogen), or vacuum conditions, to prevent oxidation, contamination, or unwanted chemical reactions during heating. The furnace typically consists of a high-temperature-resistant box chamber, heating elements, and a gas supply system. Advanced models may include programmable temperature controllers, uniform heating zones, and safety interlocks to ensure operational reliability.

What Are The Key Features Of A Horizontal Vacuum Furnace?

Key features include: 1. Heating materials at extremely high temperatures with low pollution and high consistency. 2. Capability to load materials vertically or horizontally. 3. Options for batch or continuous designs based on cooling medium, load size, temperature, and pressure. 4. Hot wall and cold wall designs, with cold wall furnaces offering higher operating temperature ranges, faster heating and cooling, and greater temperature uniformity. 5. Precise control over temperature, pressure, and atmosphere, integrating high-quality materials and advanced systems for durability, efficiency, and reliability.

What Are The Main Applications Of Vacuum Induction Furnaces?

Vacuum induction furnaces are widely used in industries such as aerospace, metallurgy, and materials research for processes like melting, sintering, heat treatment, and brazing of metals and alloys. They are particularly useful for producing high-purity metals and advanced materials.

How Does A Vacuum Furnace Work?

The working principle of a vacuum furnace involves removing air and gases from the chamber to create a vacuum, which prevents oxidation and contamination. Heating elements generate heat, and a temperature control system regulates the heating process to ensure precise and consistent results. The vacuum system pumps the furnace chamber to create a vacuum, and the heating element then heats the chamber while the temperature control system regulates heating speed and holding time, allowing materials to be heated under vacuum conditions.

How Does An Atmosphere Furnace Work?

A tube furnace generates heat through a heat source and transfers this heat to the heated workpiece or medium via the furnace tube. This process provides stable and uniform heating suitable for various industrial applications. The principle of sintering involves heating materials to high temperatures below their melting points, causing particles to bond and form a solid structure. Heat and sometimes pressure are applied to compact and densify materials, enhancing their mechanical and physical properties.

How Does A Horizontal Vacuum Furnace Work?

The working principle involves: 1. Removing air and gases from the chamber to create a vacuum, which prevents oxidation and contamination. 2. Heating elements generate heat, and a temperature control system regulates the heating process to ensure precise and consistent results. 3. The vacuum system pumps the furnace chamber to create a vacuum, and the heating element heats the chamber while the temperature control system regulates heating speed and holding time, allowing materials to be heated under vacuum conditions.

How Does A Vacuum Induction Furnace Work?

The furnace operates by creating a vacuum in the chamber to remove air and gases, preventing oxidation. Induction heating is then used to melt the metals. This combination of vacuum and induction heating ensures a clean, controlled environment for high-quality metal processing.

What Are The Advantages Of Using A Vacuum Furnace?

The benefits of a vacuum furnace include precise temperature control within a small area, low contamination of the product by carbon, oxygen, and other gases, quick cooling (quenching) of the product, and computer-controlled processes to ensure metallurgical repeatability. Additionally, vacuum furnaces provide a highly pure processing environment, fast processing speed due to no need for atmosphere adjustment, and strong controllability of the processing process as it is not affected by the atmosphere.

What Are The Advantages Of Using An Atmosphere Furnace?

The advantages of an atmosphere furnace include strong environmental control capability by adjusting atmosphere components, lower cost compared to vacuum furnaces, and a wide range of applications suitable for various materials like metals and ceramics. Additionally, atmosphere tube furnaces offer precise temperature control, flexible atmosphere control, high heating efficiency, energy conservation and environmental protection, safe and reliable operation, wide applicability, and reasonable structural design.

What Are The Advantages Of Using A Horizontal Vacuum Furnace?

Advantages include: 1. Contamination-Free Environment: The vacuum eliminates oxygen and other reactive gases, preventing oxidation and contamination. 2. Precision: Temperature control systems ensure consistent and accurate heating. 3. Versatility: Suitable for a wide range of materials and processes. 4. Efficiency: Minimizes heat loss and energy consumption due to the vacuum environment. Additional benefits are controllable temperature range, uniform temperature between 1100-1500°C, low product contamination by gases, rapid quenching cooling, computer-controlled processes for metallurgical repeatability, and prevention of high-temperature oxidation. The vacuum environment also minimizes oxidation and decarburization for cleaner surfaces and material integrity.

What Are The Advantages Of Using A Vacuum Induction Furnace?

Key advantages include: 1. Contamination-free processing due to the absence of oxygen and reactive gases. 2. Precise temperature control for consistent results. 3. Versatility in handling various materials and processes. 4. High efficiency with minimal heat loss. 5. Improved product quality by removing impurities.

What Types Of Materials Can Be Processed In A Vacuum Furnace?

Vacuum furnaces are primarily used for processing metals, including sintering, annealing, and brazing. They are also suitable for ceramics, composites, and other advanced materials, especially in applications requiring high purity and precise temperature control, such as semiconductor devices, optical thin films, and nanomaterials.

What Types Of Gases Can Be Used In An Atmosphere Furnace?

An atmosphere furnace can maintain specific gas environments such as inert gases (e.g., nitrogen, argon), reducing gases (e.g., hydrogen), or vacuum conditions to prevent oxidation, contamination, or unwanted chemical reactions during heating.

What Types Of Materials Can Be Processed In A Horizontal Vacuum Furnace?

Horizontal vacuum furnaces are suitable for processing a variety of materials including metals, alloys, electronic components, composite materials, and ceramics. They are particularly effective for materials that require high-temperature treatments without oxidation or contamination.

What Types Of Vacuum Induction Furnaces Are Available?

Vacuum induction furnaces come in various designs including batch or continuous types, and hot wall or cold wall configurations. They can also be customized based on cooling medium, load size, temperature requirements, and pressure conditions to suit specific industrial or research needs.

What Is The Difference Between Hot Wall And Cold Wall Vacuum Furnaces?

Hot wall vacuum furnaces have the heating elements and insulation inside the vacuum chamber, while cold wall furnaces have these components outside the chamber. Cold wall furnaces offer higher operating temperature ranges, faster heating and cooling, and greater temperature uniformity compared to hot wall designs.

What Safety Features Are Available In Advanced Atmosphere Furnaces?

Advanced atmosphere furnaces may include programmable temperature controllers, uniform heating zones, and safety interlocks to ensure operational reliability. A program-controlled atmosphere furnace includes a protection system that monitors critical parameters such as furnace temperature and oxygen content. In case of any abnormalities, the system can automatically shut down or trigger an alarm to protect both the furnace and the samples inside.

What Is The Temperature Range Of A Horizontal Vacuum Furnace?

Horizontal vacuum furnaces typically offer a controllable temperature range, with uniform temperatures achievable between 1100-1500°C. Some models can reach even higher temperatures, up to 2200°C or more, depending on the design and application requirements.

Why Is Temperature Control Important In Vacuum Induction Furnaces?

Precise temperature control is crucial to ensure uniform heating, prevent material degradation, and achieve consistent results in processes like melting, sintering, or heat treatment. Advanced control systems in these furnaces maintain accurate temperatures throughout the process.

Can Vacuum Furnaces Be Customized For Specific Applications?

Yes, vacuum furnaces can be customized based on cooling medium, load size, temperature, and pressure requirements. They can be designed as batch or continuous systems and can be tailored for specific applications such as sintering, brazing, or heat treatment, with options for vertical or horizontal loading.

What Materials Can Be Processed In A Vacuum Induction Furnace?

These furnaces can process a wide range of materials including metals, alloys, ceramics, and composites. They are particularly effective for materials that require high purity or are sensitive to oxidation, such as titanium, nickel-based alloys, and rare earth metals.

How Does The Vacuum Environment Benefit Material Processing?

The vacuum environment eliminates oxygen and other reactive gases, preventing oxidation and contamination of materials. It also allows for better control of the processing atmosphere, reduces heat loss, and enables higher temperature operations without material degradation.
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4.9

out of

5

Incredible precision and durability—this furnace outperforms competitors effortlessly!

Elara Voss

4.8

out of

5

Fast delivery and top-notch quality. Worth every penny!

Rafael Mendoza

4.7

out of

5

The technological advancement in this furnace is mind-blowing. Highly recommend!

Anika Patel

4.9

out of

5

Exceptional build quality and efficiency. A game-changer for our lab!

Lars Bjornsson

4.8

out of

5

Reliable and consistent performance. Perfect for high-temperature applications.

Yuki Tanaka

4.9

out of

5

The furnace arrived sooner than expected and works flawlessly. Impressed!

Isabella Moretti

4.7

out of

5

Great value for money. The furnace handles heavy use without issues.

Dmitri Volkov

4.8

out of

5

Superior heat treatment results with minimal energy consumption. Love it!

Sophie Laurent

4.9

out of

5

The durability of this furnace is unmatched. A solid investment!

Carlos Rios

4.8

out of

5

Easy to operate and maintain. Perfect for our production needs.

Nia Johnson

4.9

out of

5

Cutting-edge technology with reliable performance. A must-have!

Hiroshi Yamamoto

4.7

out of

5

Fast shipping and excellent customer service. The furnace is a beast!

Elena Petrov

4.8

out of

5

Consistent results every time. This furnace is a workhorse!

Marcus Lee

4.9

out of

5

The precision and control are outstanding. Worth every cent!

Aisha Khan

4.8

out of

5

High-quality materials and superb craftsmanship. Very satisfied!

Luca Ferrari

4.7

out of

5

Efficient and reliable. Perfect for our research projects.

Freya Olsen

4.9

out of

5

The furnace’s performance exceeds expectations. A stellar product!

Rajiv Kapoor

4.8

out of

5

Quick setup and incredible results. This furnace is a winner!

Clara Schmidt

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Molybdenum Vacuum Heat Treat Furnace

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